Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In- situ characterization of Renaissance plates by portable micro-Raman and XRF (Articolo in rivista)

Type
Label
  • Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In- situ characterization of Renaissance plates by portable micro-Raman and XRF (Articolo in rivista) (literal)
Anno
  • 2011-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.1002/jrs.2699 (literal)
Alternative label
  • Rosi F., Manuali V., Grygar T., Bezdicka P., Brunetti B.G., Sgamellotti A., Burgio L., Seccaroni C., Miliani C. (2011)
    Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In- situ characterization of Renaissance plates by portable micro-Raman and XRF
    in Journal of Raman spectroscopy
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Rosi F., Manuali V., Grygar T., Bezdicka P., Brunetti B.G., Sgamellotti A., Burgio L., Seccaroni C., Miliani C. (literal)
Pagina inizio
  • 407 (literal)
Pagina fine
  • 414 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 42 (literal)
Rivista
Note
  • ISI Web of Science (WOS) (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • INSTM Operative Unit of Perugia c/o Dipartimento di Chimica, Università di Perugia Centro di Eccellenza SMAArt (ScientificMethodologies applied to Archaeology andArt), c/oDipartimentodi Chimica, Università degli Studi di Perugia Institute of Inorganic Chemistry of the ASCR, v.v.i, 250 68 Rez, Czech Republic Institute of Inorganic Chemistry of the ASCR, v.v.i, 250 68 Rez, Czech Republic Centro di Eccellenza SMAArt (ScientificMethodologies applied to Archaeology andArt), c/oDipartimentodi Chimica, Università degli Studi di Perugia Centro di Eccellenza SMAArt (ScientificMethodologies applied to Archaeology andArt), c/oDipartimentodi Chimica, Università degli Studi di Perugia Conservation Department, Science Section, Victoria and AlbertMuseum, South Kensington, London SW7 2RL, UK ENEA (Italian National Agency for New Technologies, Energy and Sustainable Economic Development), Casaccia Research Centre IstitutoCNR-ISTM(Istitutodi Scienze eTecnologieMolecolari), c/o Dipartimento di Chimica, Università degli Studi di Perugia, (literal)
Titolo
  • Raman scattering features of lead pyroantimonate compounds: implication for the non-invasive identification of yellow pigments on ancient ceramics. Part II. In- situ characterization of Renaissance plates by portable micro-Raman and XRF (literal)
Abstract
  • The effectiveness of Raman spectroscopy (using a bench-top system on standard pigments) for the characterisation of modified lead antimonate yellowswasdemonstrated inthealreadypublishedPart I.Theknowledgegained is employedhere for the study of yellow glazes on genuine Renaissance plates with the aim of identifying non-invasively lead pyroantimonate compounds by portable micro-Raman equipment. The investigation was carried out directly on site, at the Victoria and Albert Museum (London, UK) and at the Museo Statale d'Arte Medievale di Arezzo (Arezzo, Italy), combining Raman and X-ray fluorescence analyses. In addition to the spectral features of both unmodified Naples yellow and Sn- and Zn-modified lead antimonate compounds, the Raman patterns related to partially modified pyrochlore structureswere observed. For this reason, the possible Sn-induced modification of Naples yellow by cassiterite (SnO2), present within the glaze as opacifier was explored on lead antimonate yellow glazemock-ups fired at different temperatures. (literal)
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