Survey of T-2 and HT-2 toxins in soybean and soy meal from Argentina using immunoaffinity clean up and high performance liquid chromatography. (Articolo in rivista)

Type

• Articolo in rivista (Classe)
• Prodotto della ricerca (Classe)

Label

• Survey of T-2 and HT-2 toxins in soybean and soy meal from Argentina using immunoaffinity clean up and high performance liquid chromatography. (Articolo in rivista) (literal)

Anno

• 2011-01-01T00:00:00+01:00 (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi

• 10.3920/WMJ2010.1272 (literal)

Alternative label

• Barros G., Garcìa D., Oviedo M.S., Ramirez M.L., Torres A., Lattanzio V., Pascale M., Chulze S.N. (2011)
  Survey of T-2 and HT-2 toxins in soybean and soy meal from Argentina using immunoaffinity clean up and high performance liquid chromatography.
  in World mycotoxin journal (Print)
  (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori

• Barros G., Garcìa D., Oviedo M.S., Ramirez M.L., Torres A., Lattanzio V., Pascale M., Chulze S.N. (literal)

Pagina inizio

• 189 (literal)

Pagina fine

• 197 (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume

• 4 (literal)

Rivista

• World mycotoxin journal (Rivista)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroFascicolo

• 2 (literal)

Note

• ISI Web of Science (WOS) (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni

• Departamento de Microbiología e Inmunología, Facultad de Ciencias Exactas Físico Químicas y Naturales, Universidad Nacional de Río Cuarto, Ruta Nacional 36 Km 601, 5800 Río Cuarto, Córdoba, Argentina; Member of the Research Career of CONICET, Argentina; National Research Council, Institute of Sciences of Food Production CNR- ISPA, Via G. Amendola 122/O, 70126 Bari, Italy (literal)

Titolo

• Survey of T-2 and HT-2 toxins in soybean and soy meal from Argentina using immunoaffinity clean up and high performance liquid chromatography. (literal)

Abstract

• Soybean and soy meal samples collected during the harvest season 2008-2009 in the soybean-growing area of Córdoba Province in Argentina were analysed for T-2 and HT-2 toxins occurrence. These mycotoxins were detected using HPLC analysis with fluorescence detection after derivatisation with 1-anthronylnitrile and immunoaffinity column clean-up. Characteristics of in-house validated method such as accuracy, precision, detection and quantification limits were defined by means of recovery test with spiked soybean and soy meal samples. Mean recoveries for T-2 within the spiking range 125-500 ?g/kg, were 90.9 and 81.3% for soybean and soy meal, respectively with a within-laboratory relative standard deviation <10%. Analysis of samples spiked with HT-2 in the same range gave a mean recovery of 70.2 and 77.5% for soybean and soy meal, respectively, with relative standard deviations <12%. The limit of detection for the method was 25 ?g/kg for T-2 and HT-2, based on a signal-to-noise ratio 3:1 and the limit of quantification was established as three times the detection limit. Out of 64 samples, only two soybean samples showed contamination with A-type trichothecenes evaluated. Confirmatory analyses of the contaminated samples were performed by LC-MS/MS. This study demonstrated low incidences and levels of T-2 and HT-2 in soybean harvested among the areas in the Cordoba Province. (literal)

Prodotto di

• Istituto di scienze delle produzioni alimentari (ISPA) (Istituto)
• Metodi innovativi per l'analisi e la riduzione di micotossine, funghi tossigeni ed allergeni nei prodotti agroalimentari (AG.P05.008.002) (Modulo)

Autore CNR

• MICHELANGELO PASCALE (Unità di personale interno)
• VERONICA MARIA TERESA LATTANZIO (Unità di personale interno)

Incoming links:

Prodotto

• Istituto di scienze delle produzioni alimentari (ISPA) (Istituto)
• Metodi innovativi per l'analisi e la riduzione di micotossine, funghi tossigeni ed allergeni nei prodotti agroalimentari (AG.P05.008.002) (Modulo)

Autore CNR di

• MICHELANGELO PASCALE (Unità di personale interno)
• VERONICA MARIA TERESA LATTANZIO (Unità di personale interno)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#rivistaDi

• World mycotoxin journal (Rivista)