http://www.cnr.it/ontology/cnr/individuo/prodotto/ID45871
Quantitation of lysinoalanine in dairy products by liquid chromatography-mass spectrometry with selective ion monitoring (Articolo in rivista)
- Type
- Label
- Quantitation of lysinoalanine in dairy products by liquid chromatography-mass spectrometry with selective ion monitoring (Articolo in rivista) (literal)
- Anno
- 2009-01-01T00:00:00+01:00 (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
- 10.1016/j.foodchem.2009.03.041 (literal)
- Alternative label
Calabrese MG; Mamone G, Caira S, Ferranti P, Addeo F. (2009)
Quantitation of lysinoalanine in dairy products by liquid chromatography-mass spectrometry with selective ion monitoring
in Food chemistry
(literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
- Calabrese MG; Mamone G, Caira S, Ferranti P, Addeo F. (literal)
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- http://www.isa.cnr.it (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
- Rivista
- Note
- ISI Web of Science (WOS) (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
- Institute of Food Science, National Research Council, via Roma 64, 83100 Avellino, Italy
Department of Food Science, University of Naples Federico II, Parco Gussone, 80055 Portici (Napoli), Italy (literal)
- Titolo
- Quantitation of lysinoalanine in dairy products by liquid chromatography-mass spectrometry with selective ion monitoring (literal)
- Abstract
- The unnatural amino acid lysinoalanine (LAL) has been identified in milk and cheese products by liquid
chromatography mass spectrometry (LC/ESI/MS) with selective ion monitoring (SIM) of the 9-fluorenylmethylchloro-
formate (FMOC) derivative. LAL is not present in raw milk or derived from Mozzarella
cheese; however, high amounts of LAL are found in calcium caseinate and milk powder. As expected, milk
fortified with caseinate or whey protein powder produces cheese with higher LAL content. Our analytical
procedure is based on the simultaneous detection of specific ion masses of the FMOCLAL derivative and
the N-e-methyl-lysine internal standard. A linear relationship was observed within the 0.220 ppm concentration
range, in addition to a high correlation coefficient and 3% relative standard deviation. (literal)
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