High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide (Articolo in rivista)

Type
Label
  • High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide (Articolo in rivista) (literal)
Anno
  • 2005-01-01T00:00:00+01:00 (literal)
Alternative label
  • Roiebben, O. Van der Biest, D. Sciti, A. Bellosi, C. Sarbu, T. Lauwagie (2005)
    High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide
    in Journal of the American Ceramic Society
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Roiebben, O. Van der Biest, D. Sciti, A. Bellosi, C. Sarbu, T. Lauwagie (literal)
Pagina inizio
  • 2152 (literal)
Pagina fine
  • 2158 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 88 (literal)
Rivista
Note
  • ISI Web of Science (WOS) (literal)
Titolo
  • High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide (literal)
Abstract
  • The Impulse Excitation Technique was used to determine stiffness and internal friction (Q-1) of liquid-phase sintered silicon carbide (LPS-SiC) up to 1400°C. As-hot-pressed materials display a stable Q 1-peak near 1100°C, superimposed on an exponentially increasing background. The stiffness loss associated with the Q-1-peak is quantitatively related to the amount of amorphous intergranular matter, providing a new methodology for assessing this critical microstructural parameter. The background damping is related to the grain boundary sliding resistance, and indicative of the elevated temperature flexural strength. Annealing at 1900°C for 3 hours eliminates the amorphous intergranular volumes, as observed with TEM and deduced from the absence of a Q 1-peak with associated stiffness loss, and successfully increases the high temperature strength. (literal)
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