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High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide (Articolo in rivista)
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- High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide (Articolo in rivista) (literal)
- Anno
- 2005-01-01T00:00:00+01:00 (literal)
- Alternative label
Roiebben, O. Van der Biest, D. Sciti, A. Bellosi, C. Sarbu, T. Lauwagie (2005)
High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide
in Journal of the American Ceramic Society
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- Roiebben, O. Van der Biest, D. Sciti, A. Bellosi, C. Sarbu, T. Lauwagie (literal)
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- Titolo
- High-temperature stiffness and damping measurements to monitor the glassy intergranular phase in liquid phase sintered silicon carbide (literal)
- Abstract
- The Impulse Excitation Technique was used to determine stiffness and internal friction (Q-1) of liquid-phase sintered silicon carbide (LPS-SiC) up to 1400°C. As-hot-pressed materials display a stable Q 1-peak near 1100°C, superimposed on an exponentially increasing background. The stiffness loss associated with the Q-1-peak is quantitatively related to the amount of amorphous intergranular matter, providing a new methodology for assessing this critical microstructural parameter. The background damping is related to the grain boundary sliding resistance, and indicative of the elevated temperature flexural strength. Annealing at 1900°C for 3 hours eliminates the amorphous intergranular volumes, as observed with TEM and deduced from the absence of a Q 1-peak with associated stiffness loss, and successfully increases the high temperature strength. (literal)
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