Synthesis and characterization of optically transparent epoxy matrix nanocomposites (Articolo in rivista)

Type
Label
  • Synthesis and characterization of optically transparent epoxy matrix nanocomposites (Articolo in rivista) (literal)
Anno
  • 2009-01-01T00:00:00+01:00 (literal)
Alternative label
  • Corcione CE, Manera MG, Maffezzoli A, Rella R (2009)
    Synthesis and characterization of optically transparent epoxy matrix nanocomposites
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Corcione CE, Manera MG, Maffezzoli A, Rella R (literal)
Pagina inizio
  • 1798 (literal)
Pagina fine
  • 1802 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 29 (literal)
Note
  • ISI Web of Science (WOS) (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • 1. Dipartimento Ingn Innovaz, I-73100 Lecce, Italy 2. IMM, CNR, Sez Lecce, I-73100 Lecce, Italy (literal)
Titolo
  • Synthesis and characterization of optically transparent epoxy matrix nanocomposites (literal)
Abstract
  • In this work optically transparent nanocomposites were prepared and characterized from an optical and morphological point of view. An organically modified boehmite was added at different concentrations in a diglycidyl ether of bisphenol A (DGEBA) epoxy matrix, hardened with a polyether diamine. Nanocomposites were characterized structurally by X-ray diffraction (XRD), optically by UV-Vis-NIR spectrophotometry and their morphology was investigated by Atomic Force Microscopy (AFM). Morphological investigation reveals the presence of boehmite particles dispersed in the epoxy matrix in different dimensions ranging from ten to hundreds of nanometers; some aggregation in the particles is the tendency noticed in the AFM images. The acquisition of multiple AFM images in different areas of the sample was used for a statistical analysis of the volumetric distribution of boehmite aggregates. The obtained result, (3.6 +/- 0.3)%vol, is well comparable to thermogravimetric analysis. (literal)
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