Description of a flexible cell for in situ X-ray and far-IR characterization of the surface of powdered materials (Articolo in rivista)

Type
Label
  • Description of a flexible cell for in situ X-ray and far-IR characterization of the surface of powdered materials (Articolo in rivista) (literal)
Anno
  • 2003-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.1016/S0168-583X(02)01719-6 (literal)
Alternative label
  • Lamberti, C (Lamberti, C); Prestipino, C (Prestipino, C); Bordiga, S (Bordiga, S); Berlier, G (Berlier, G); Spoto, G (Spoto, G); Zecchina, A (Zecchina, A); Laloni, A (Laloni, A); La Manna, F (La Manna, F); D'Anca, F (D'Anca, F); Felici, R (Felici, R); D'Acapito, F (D'Acapito, F); Roy, P (Roy, P) (2003)
    Description of a flexible cell for in situ X-ray and far-IR characterization of the surface of powdered materials
    in Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms (Print)
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Lamberti, C (Lamberti, C); Prestipino, C (Prestipino, C); Bordiga, S (Bordiga, S); Berlier, G (Berlier, G); Spoto, G (Spoto, G); Zecchina, A (Zecchina, A); Laloni, A (Laloni, A); La Manna, F (La Manna, F); D'Anca, F (D'Anca, F); Felici, R (Felici, R); D'Acapito, F (D'Acapito, F); Roy, P (Roy, P) (literal)
Pagina inizio
  • 196 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 200 (literal)
Rivista
Note
  • ISI Web of Science (WOS) (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • CNR, INFM (literal)
Titolo
  • Description of a flexible cell for in situ X-ray and far-IR characterization of the surface of powdered materials (literal)
Abstract
  • We have designed and realized a cell where a powdered sample, in form of self-supported pellet, can be (i) in situ heated up to 900 K, either under dynamical vacuum or in reducing/oxidizing atmosphere; (ii) contacted with the desired amount of adsorbed gas; (iii) cooled down to 77 K for measurements. The cell (transmission geometry) has been employed in X-ray absorption experiments at LURE DCI (EXAFS13) and ESRF (GILDA BN18 and ID24), in far-IR experiments at LURE Super-ACO (SIRLOIN) and in conventional mid-IR experiments in our laboratory, only by changing the windows (mylar, silicon and KBr, respectively). A brief overview on the results obtained with this cell is reported to illustrate the potentialities of the instrument. Literature. is quoted to allow possible in-depth study (literal)
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