http://www.cnr.it/ontology/cnr/individuo/prodotto/ID219339
Increasing the large scale feasibility of a solid phase extraction procedure for the recovery of natural antioxidants from olive mill wastewaters (Articolo in rivista)
- Type
- Label
- Increasing the large scale feasibility of a solid phase extraction procedure for the recovery of natural antioxidants from olive mill wastewaters (Articolo in rivista) (literal)
- Anno
- 2012-01-01T00:00:00+01:00 (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
- 10.1016/j.cej.2012.05.079 (literal)
- Alternative label
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
- Alberto Scoma; Cristina Pintucci; Lorenzo Bertin; Pietro Carlozzi; Fabio Fava (literal)
- Pagina inizio
- Pagina fine
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#url
- http://dx.doi.org/10.1016/j.cej.2012.05.079 (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
- Rivista
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#pagineTotali
- Note
- ISI Web of Science (WOS) (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
- DICAM, Unit of Environmental Biotechnology and Biorefineries, Faculty of Engineering, University of Bologna, via Terracini 28, 40131 Bologna, Italy
ISE, CNR, Institute for the Study of the Ecosystems, National Council of Research, via Madonna del piano 10, 50012 Sesto Fiorentino (FI), Italy
INCA - Interuniversitary Consortium ''Chemistry for the Environment'', via delle Industrie 21/8, 30175 Marghera (VE), Italy (literal)
- Titolo
- Increasing the large scale feasibility of a solid phase extraction procedure for the recovery of natural antioxidants from olive mill wastewaters (literal)
- Abstract
- The present investigation was focused on improving the feasibility of large scale applications of a solid
phase extraction (SPE) procedure dedicated to the recovery of polyphenols from olive mill wastewaters
(OMWs). To this aim, a previously developed SPE procedure was optimized in terms of contact time without
negatively affecting the overall process productivity. The possibility of regenerating and recycling
both the solid phase (Amberlite XAD16 non-polar resin) and the extraction solvent (acidified ethanol)
was also demonstrated. In particular, the resin was successfully reused in 10 consecutive SPE cycles
(including washing and reactivation steps), allowing almost constant polyphenols adsorption and
desorption ratios (81.44 ± 0.91% and 52.69 ± 5.57%, respectively). Up to 695 mL of ethanol per liter of
exhausted extraction solvent were recovered by means of a rotary evaporator. Furthermore, the solvent
conventionally used for resin activation (i.e., methanol) was successfully substituted by a more biocompatible
solvent (i.e., ethanol). An ORAC value corresponding to 6979 lM of Trolox equivalents was
observed for the concentrated polyphenolic solution, obtained as a result of rotary evaporator operations.
Importantly, no substantial loss of radical scavenging and antioxidant activities occurred by means of the
aforementioned operations dedicated to the recovery of ethanol from the obtained polyphenolic solution. (literal)
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