http://www.cnr.it/ontology/cnr/individuo/prodotto/ID191159
Mechanisms of Reactions in the Solid State: (110) Al2O3 + (001) ZnO Interfacial Reaction. (Articolo in rivista)
- Type
- Label
- Mechanisms of Reactions in the Solid State: (110) Al2O3 + (001) ZnO Interfacial Reaction. (Articolo in rivista) (literal)
- Anno
- 2012-01-01T00:00:00+01:00 (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
- 10.1021/jp209622u (literal)
- Alternative label
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
- Pin S.; Newton M.A.; D'Acapito F.; Zema M.; Tarantino S.C.; Spinolo G.; De Souza R. A.; Martin M.; Ghigna P. (literal)
- Pagina inizio
- Pagina fine
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#url
- http://pubs.acs.org/doi/abs/10.1021/jp209622u (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
- Rivista
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- ISI Web of Science (WOS) (literal)
- Scopu (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
- 1,6,9 : INSTM, IENI/CNR, Università di Pavia, I27100 Pavia, Italy /
2 : ESRF, BP 220, F-38043 Grenoble Cedex, France /
3 : GILDA-CRG, ESRF, BP 220, F-38043 Grenoble Cedex, France /
4,5 : Dipartimento di Scienze della Terra e dell'Ambiente, Università di Pavia, I27100 Pavia, Italy /
7,8 : Institute of Physical Chemistry, RWTH Aachen University, Landoltweg 2, 52056 Aachen, Germany /
1 : Paul Scherrer Institut, 5232 Villigen PSI, Switzerland (literal)
- Titolo
- Mechanisms of Reactions in the Solid State: (110) Al2O3 + (001) ZnO Interfacial Reaction. (literal)
- Abstract
- The mechanisms of the (110) Al 2O 3 + (001) ZnO interfacial reaction, that eventually yields the spinel ZnAl 2O 4, has been studied using a multitechnique approach involving local- and long-range structural probes (EXAFS, ?-XANES, and XRPD) and a surface analytical probe such as SIMS. It is demonstrated that the reaction involves a series of different steps, where at least two different nonequilibrium compounds are formed and then transformed into the spinel. One of these compounds, playing a role similar to reactive intermediates in solution chemistry, has been trapped. To the best of our knowledge, this is the first time that such a kind of behavior has been demonstrated for a heterogeneous solid state reaction. It is argued that the critical step is a concerted, homogeneous movement of a set of atoms, rather than long-range diffusion. The implications of these findings for the fabrication of ceramic and nanoscale materials are discussed. (literal)
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