A Rapid Liquid Chromatography Electrospray Ionization Mass Spectrometry(n) method for evaluation of synephrine in Citrus aurantium L. samples (Articolo in rivista)

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  • A Rapid Liquid Chromatography Electrospray Ionization Mass Spectrometry(n) method for evaluation of synephrine in Citrus aurantium L. samples (Articolo in rivista) (literal)
Anno
  • 2005-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.1021/jf051270+ (literal)
Alternative label
  • LUISA MATTOLI; FRANCESCA CANGI; ANNA MAIDECCHI; CATERINA GHIARA; MICHELA TUBARO ;PIETRO TRALDI (2005)
    A Rapid Liquid Chromatography Electrospray Ionization Mass Spectrometry(n) method for evaluation of synephrine in Citrus aurantium L. samples
    in Journal of agricultural and food chemistry; ACS, American chemical society, Washington, DC (Stati Uniti d'America)
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • LUISA MATTOLI; FRANCESCA CANGI; ANNA MAIDECCHI; CATERINA GHIARA; MICHELA TUBARO ;PIETRO TRALDI (literal)
Pagina inizio
  • 9860 (literal)
Pagina fine
  • 9866 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#url
  • http://pubs.acs.org/doi/abs/10.1021/jf051270%2B (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 53 (literal)
Rivista
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroFascicolo
  • 26 (literal)
Note
  • Scopu (literal)
  • ISI Web of Science (WOS) (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • 1-4 : Chemical and Pharmacological Research Area, Aboca S.p.A., Aboca 20, Sansepolcro (AR), Italy, and 5-6 : CNR-ISTM, Area di Ricerca, Corso Stati Uniti 4, 35127, Padova, Italy (literal)
Titolo
  • A Rapid Liquid Chromatography Electrospray Ionization Mass Spectrometry(n) method for evaluation of synephrine in Citrus aurantium L. samples (literal)
Abstract
  • Immature bitter orange fruit and its extracts have been introduced into the market as an alternative to Ephedra in weight loss products. However, the safety of the immature bitter orange fruit and its extracts is a debated argument due to the presence of synephrine, a constituent known as a sympathomimetic agent. In this paper, we describe the development of a new, rapid, and simple liquid chromatography-electrospray ionization-tandem mass spectrometry method devoted to the quantitative determination of synephrine in bitter orange samples, containing a high quantity of synephrine, and sweet orange samples, known to contain a low level of synephrine but at the same time being one of the main synephrine sources in a normal human diet. Two bitter orange dry extracts containing 5 and 6% sSynephrine and 10 sweet orange samples have been analyzed. Between the sweet orange samples, six were fresh oranges and four were fresh-squeezed juices; in these samples, the synephrine levels ranged from 0.00128 to 0.00349%. (literal)
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