http://www.cnr.it/ontology/cnr/individuo/prodotto/ID17402
Synthesis of alpha-trifluoromethyl-alpha-amino-beta-sulfone hydroxamates: novel nanomolar inhibitors of matrix metalloproteinases (Articolo in rivista)
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- Label
- Synthesis of alpha-trifluoromethyl-alpha-amino-beta-sulfone hydroxamates: novel nanomolar inhibitors of matrix metalloproteinases (Articolo in rivista) (literal)
- Anno
- 2005-01-01T00:00:00+01:00 (literal)
- Alternative label
Sinisi R., Sani M., Candiani G., Parente R., Pecker F., Bellosta S., Zanda M. (2005)
Synthesis of alpha-trifluoromethyl-alpha-amino-beta-sulfone hydroxamates: novel nanomolar inhibitors of matrix metalloproteinases
in Tetrahedron letters
(literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
- Sinisi R., Sani M., Candiani G., Parente R., Pecker F., Bellosta S., Zanda M. (literal)
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- ISI Web of Science (WOS) (literal)
- Titolo
- Synthesis of alpha-trifluoromethyl-alpha-amino-beta-sulfone hydroxamates: novel nanomolar inhibitors of matrix metalloproteinases (literal)
- Abstract
- The racemic alpha-trifluoromethyl-alpha-amino-beta-sulfone hydroxamates 1 were synthesized by means of a nucleophilic addition of sulfur-stabilized carbanions to a N-Cbz imine of trifluoropyruvate (4). The free amino derivative 1a was the most potent inhibitor of both MMP-3 (stromelysin-1) and MMP-9 (gelatinase-B), showing an IC50 = 14 nM and 1 nM, respectively, and excellent selectivity versus MMP- 1 (>5000-fold difference in inhibitory capacity). The N-Me derivative 1b was the most selective for MMP-3 with respect to MMP-9 (62-fold difference). (literal)
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