http://www.cnr.it/ontology/cnr/individuo/prodotto/ID50471
An effective and useful synthesis of enantiomerically enriched arylglycinols (Articolo in rivista)
- Type
- Label
- An effective and useful synthesis of enantiomerically enriched arylglycinols (Articolo in rivista) (literal)
- Anno
- 2001-01-01T00:00:00+01:00 (literal)
- Alternative label
Bandini, Marco; Cozzi, Pier Giorgio; Gazzano, Massimo; Umani-Ronchi, Achille (2001)
An effective and useful synthesis of enantiomerically enriched arylglycinols
in European journal of organic chemistry (Print)
(literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
- Bandini, Marco; Cozzi, Pier Giorgio; Gazzano, Massimo; Umani-Ronchi, Achille (literal)
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- In questo articolo รจ descritta la preparazione e la risoluzione della miscela racemica di arilglicinoli. (literal)
- Note
- ISI Web of Science (WOS) (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
- ISOF - CNR - Bologna
Dip. di Chimica \"G. Ciamician\", Univ. di Bologna (literal)
- Titolo
- An effective and useful synthesis of enantiomerically enriched arylglycinols (literal)
- Abstract
- A two-step synthesis of racemic arylglycinols, together with a simple and straightforward methodol. for their resoln., is described. This method constitutes a practical means of prepg. racemic and optically pure electron-rich or electron-poor substituted arylglycinols, useful building blocks for the synthesis of biol. active mols. and chiral ligands. All of the chiral beta-amino alcs. were isolated in good chem. yields and with excellent enantiomeric excesses. Chiral fluoroarom. vicinal amino alcs. can also be obtained with good enantiopurity using such a procedure. The key step of the strategy presented is an easy chromatog. sepn. of the diastereoisomeric amides prepd. from acetyl mandeloyl chloride. The abs. configuration of the perfluorinated amino alcs. was detd. by X-ray anal. of the corresponding amide. (literal)
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