http://www.cnr.it/ontology/cnr/individuo/prodotto/ID40100
Generation of volatile cobalt species by UV photoreduction and their tentative identification (Articolo in rivista)
- Type
- Label
- Generation of volatile cobalt species by UV photoreduction and their tentative identification (Articolo in rivista) (literal)
- Anno
- 2008-01-01T00:00:00+01:00 (literal)
- Alternative label
Grinberg P., Mester Z., Sturgeon R.E., Ferretti A. (2008)
Generation of volatile cobalt species by UV photoreduction and their tentative identification
in Journal of analytical atomic spectrometry (Print)
(literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
- Grinberg P., Mester Z., Sturgeon R.E., Ferretti A. (literal)
- Pagina inizio
- Pagina fine
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
- Rivista
- Note
- ISI Web of Science (WOS) (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
- Institute for National Measurements Standards, National Research
Council Canada, Ottawa, Ontario, Canada (literal)
- Titolo
- Generation of volatile cobalt species by UV photoreduction and their tentative identification (literal)
- Abstract
- Generation of volatile cobalt carbonyl was accomplished by exposing a solution of inorganic cobalt, containing low molecular weight organic acids, to UV irradiation. The gaseous products were removed from the liquid phase in a gas-liquid separator and transported to a Pyrex U-tube cryogenic trap. Following cryocondensation of the products using a dry ice-acetone bath, the U- tube was placed in a hot water bath (35-40 degrees C) and the trapped species were introduced to an ICP-MS for estimation of the efficiency of generation. Alternatively, the gas phase containing the Co species was sampled with a gastight syringe and injected into a GC-MS for species identification. The product, which is stable for periods in excess of 60 minutes, is tentatively identified as a carbonylated cobalt species, generated with an efficiency of 0.3-0.4% (literal)
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- Autore CNR
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