Preparation and characterization of porous and nonporous polymeric microspheres by the phase inversion process (Articolo in rivista)

Type

• Prodotto della ricerca (Classe)
• Articolo in rivista (Classe)

Label

• Preparation and characterization of porous and nonporous polymeric microspheres by the phase inversion process (Articolo in rivista) (literal)

Anno

• 2012-01-01T00:00:00+01:00 (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi

• 10.1002/adv.21281 (literal)

Alternative label

• Lakshmi, D.S., Figoli, A., Buonomenna, M.G., Golemme, G., Drioli, E (2012)
  Preparation and characterization of porous and nonporous polymeric microspheres by the phase inversion process
  in Advances in polymer technology (Print)
  (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori

• Lakshmi, D.S., Figoli, A., Buonomenna, M.G., Golemme, G., Drioli, E (literal)

Pagina inizio

• 231 (literal)

Pagina fine

• 241 (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume

• 31 (literal)

Rivista

• Advances in polymer technology (Rivista)

Note

• ISI Web of Science (WOS) (literal)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni

• Institute of Membrane Technology, ITM-CNR, via P. Bucci 17/c, I-87030 Rende (CS), Italy Department of Chemical Engineering and Materials, INSTM Consortium, University of Calabria, via P. Bucci, I-87030 Rende (CS), Italy (literal)

Titolo

• Preparation and characterization of porous and nonporous polymeric microspheres by the phase inversion process (literal)

Abstract

• Microspheres (MCs) of different polymers, such as poly(ether sulfone) (PES), polyetheretherketone with card, with and without pore formers, were prepared by the non-solvent-induced phase separation (NIPS) process. The polymers were solubilized in different types of solvents, such as dimethyl formamide (DMF), dimethylsulfoxide (DMSO), N-methylpyrrolidone, and ?-butyrolactone as a dispersed phase, whereas dodecane, isopropanol, water, and sodium dodecyl sulfate were used as continuous phases. The technique yielded asymmetric and symmetric porous, spongy, or finger-like, spherical MCs having a diameter tailored by the monopore film pore size employed. The influence of polymer and pore former (polyvinylpyrrolidone k17), the continuous phase composition and operating membrane process conditions, and solvent uptake behavior of different solvents are studied in detail. The operative conditions and chemical compositions are correlated with the spherical nature, structural interaction, pore size, porosity, and morphology of the MCs prepared. Ternary phase diagrams were drawn for PES/DMF and PES/DMSO using different alcohols, such as butanol, isopropanol, ethanol, and methanol. BET (Brunauer-Emmet-Teller) surface analysis also provided information about the surface of MCs. MCs with different diameters and porosities are obtained by controlling the concentration of the dispersed phase polymer concentration, used during the preparation, and diameter of the monopore film. (literal)

Prodotto di

• Sviluppo di una nuova generazione di membrane per Reattori Biologici a membrana (MBR) bioreattori a membrana (PM.P02.008.003) (Modulo)
• Institute on membrane technology (ITM) (Istituto)

Autore CNR

• ALBERTO FIGOLI (Unità di personale interno)
• SHANTHANA LAKSHMI DURAIKKANNU (Unità di personale esterno)
• ENRICO DRIOLI (Unità di personale esterno)

Insieme di parole chiave

• Parole chiave di "Preparation and characterization of porous and nonporous polymeric microspheres by the phase inversion process" (Insieme di parole chiave)

Incoming links:

Prodotto

• Institute on membrane technology (ITM) (Istituto)
• Sviluppo di una nuova generazione di membrane per Reattori Biologici a membrana (MBR) bioreattori a membrana (PM.P02.008.003) (Modulo)

Autore CNR di

• ALBERTO FIGOLI (Unità di personale interno)
• ENRICO DRIOLI (Unità di personale esterno)
• SHANTHANA LAKSHMI DURAIKKANNU (Unità di personale esterno)

Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#rivistaDi

• Advances in polymer technology (Rivista)

Insieme di parole chiave di

• Parole chiave di "Preparation and characterization of porous and nonporous polymeric microspheres by the phase inversion process" (Insieme di parole chiave)