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Thermal oxidation products of nylon 6 determined by MALDI-TOF mass spectrometry (Articolo in rivista)
- Type
- Label
- Thermal oxidation products of nylon 6 determined by MALDI-TOF mass spectrometry (Articolo in rivista) (literal)
- Anno
- 2001-01-01T00:00:00+01:00 (literal)
- Alternative label
Donatella Chionna, Concetto Puglisi, Filippo Samperi, Giorgio Montaudo, Antonio Turturro (2001)
Thermal oxidation products of nylon 6 determined by MALDI-TOF mass spectrometry
in Macromolecular rapid communications
(literal)
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- Donatella Chionna, Concetto Puglisi, Filippo Samperi, Giorgio Montaudo, Antonio Turturro (literal)
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- CNR; Universita´ di Catania; Universita´ di Genova (literal)
- Titolo
- Thermal oxidation products of nylon 6 determined by MALDI-TOF mass spectrometry (literal)
- Abstract
- Matrix-assisted laser desorption ionisation
(MALDI) mass spectrometry was used, in an attempt
to find firm evidence for the structure of the species produced
in the thermal oxidative degradation of Nylon 6
(Ny6), at 2508C in air. The MALDI spectra of the products
showed the presence of polymer chains containing
aldehydes, amides, methyl and N-formamide terminal
groups. The aldehydes undergo further oxidation to produce
carboxylic end groups. The formation of azomethines,
from the further reaction of aldehydes with
amino-terminated Ny6 chains, is also supported by the
appearance of specific peaks in the MALDI spectra. (literal)
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