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Preparation, properties and X-ray structure of a cyclic compartmental Schiff base and related complexes containing d- or f-metal ions (Articolo in rivista)
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- Preparation, properties and X-ray structure of a cyclic compartmental Schiff base and related complexes containing d- or f-metal ions (Articolo in rivista) (literal)
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- 1997-01-01T00:00:00+01:00 (literal)
- Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
- 10.1016/S0020-1693(97)05695-8 (literal)
- Alternative label
Casellato U.; Tamburini S.; Tomasin P.; Vigato P. A (1997)
Preparation, properties and X-ray structure of a cyclic compartmental Schiff base and related complexes containing d- or f-metal ions
in Inorganica Chimica Acta (Testo stamp.); ELSEVIER SCIENCE SA, PO BOX 564, 1001 LAUSANNE (Svizzera)
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- Casellato U.; Tamburini S.; Tomasin P.; Vigato P. A (literal)
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- http://www.sciencedirect.com/science/article/pii/S0020169397056958 (literal)
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- ICIS-Istituto di chimica organica e delle superfici (literal)
- Titolo
- Preparation, properties and X-ray structure of a cyclic compartmental Schiff base and related complexes containing d- or f-metal ions (literal)
- Abstract
- A new compartmental ligand (H2LA) containing an N2O2 Schiff base and an O2O4 'crown like' coordination site has been prepared by reaction of 3,3'-(3,6-dioxaoctane-1,8-diyldioxy)bis(2-hydroxybenzaldehyde) with ethylenediamine and the [1 + 1] cyclic nature was confirmed by its X-ray single crystal structural determination. When reacted with d- or f-metal ions, H2LA forms mononuclear complexes where the metal ion coordinates respectively the N2O2 or the O2O4 chamber. The X-ray structure of [La(H2LA)(H2O)(4)]Cl-3 shows the ten-coordination about the metal ion is reached by the six oxygen atoms of the compartmental ligand and by the oxygen atoms of four water molecules; the chloride atoms are ionic. (literal)
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