Synthesis and characterization of the intermetallic compound NiSbS (Articolo in rivista)

Type
Label
  • Synthesis and characterization of the intermetallic compound NiSbS (Articolo in rivista) (literal)
Anno
  • 2012-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.1007/s10973-012-2192-y (literal)
Alternative label
  • R. Carlini 1,2, ? G. Zanicchi1,2, ? G. Borzone1,2,? N. Parodi ?1,2 G. A. Costa1,3 (2012)
    Synthesis and characterization of the intermetallic compound NiSbS
    in Journal of thermal analysis and calorimetry (Print)
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • R. Carlini 1,2, ? G. Zanicchi1,2, ? G. Borzone1,2,? N. Parodi ?1,2 G. A. Costa1,3 (literal)
Pagina inizio
  • 793 (literal)
Pagina fine
  • 797 (literal)
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  • 108 (literal)
Rivista
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#pagineTotali
  • 5 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroFascicolo
  • 2 (literal)
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  • 1 DCCI, University of Genoa, Via Dodecaneso 31, 16146 Genoa, Italy 2 INSTM--Genoa Research Unit of National Consortium of Materials Science and Technology, Genoa, Italy 3 CNR-SPIN Genova, Via Dodecaneso 33, 16146 Genoa, Italy (literal)
Titolo
  • Synthesis and characterization of the intermetallic compound NiSbS (literal)
Abstract
  • The results recently obtained by our group to get new thermoelectric materials belonging to the M-Pn-Ch ternary systems (M=Co, Fe, Ni; Pn=P, As, Sb, Ch=S, Se, Te) are here reported. We have considered the Ni-Sb-S ternary system, and some homogeneous samples of composition near to 1:1:1 were prepared employing a new and simple synthetic route, starting from pure elements. Scanning electronic microscopy, electron-probe microanalysis and X-ray powder diffraction were used to investigate the microstructure. The NiSbS lattice parameters were determined and the crystal structure was refined by Rietveld method. The crystal cell of NiSbS belongs to the P213 space group with a = 0.5931 nm. The thermal stability of the ternary compounds Ni-Sb-S was investigated by DSC technique. Electrical resistivity and thermoelectric power measurements at room temperature and at 77 K were performed on platelets obtained by cleavage of the bulk. (literal)
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