X-ray microdiffraction and urine: A new analysis method of crystalluria (Articolo in rivista)

Type
Label
  • X-ray microdiffraction and urine: A new analysis method of crystalluria (Articolo in rivista) (literal)
Anno
  • 2012-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.3233/XST-2012-00355 (literal)
Alternative label
  • Baggio B., Giannossi ML., Medici L., Summa V., Tateo F. (2012)
    X-ray microdiffraction and urine: A new analysis method of crystalluria
    in Journal of X-ray science and technology (Print)
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Baggio B., Giannossi ML., Medici L., Summa V., Tateo F. (literal)
Pagina inizio
  • 489 (literal)
Pagina fine
  • 498 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 20 (literal)
Rivista
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#pagineTotali
  • 10 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroFascicolo
  • 4 (literal)
Note
  • ISI Web of Science (WOS) (literal)
  • Scopu (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • Baggio B., Giannossi ML., Medici L., Summa V., Tateo F. (literal)
Titolo
  • X-ray microdiffraction and urine: A new analysis method of crystalluria (literal)
Abstract
  • The qualitative and quantitative analyses of crystalluria have clinical significance in the diagnosis and prognosis of urolithiasis. The aim of this paper is to provide a new accurate methodology to get qualitative and quantitative data on urine particulate in patients with renal stone disease. The procedure involves a urine collection, the separation of the solid residual by centrifugation, and its analysis by X-ray diffraction, utilizing a micro-diffractometer in order to analyze very low amounts of residual. The spectrum obtained was converted into 2 I profiles and quantitatively refined by Rietveld method. The proposed methodology has the advantage to accurately quantify all crystalline phases and the amorphous component of the urine; anyway urine samples have to be centrifuged and analysed as soon as possible, because the quantitative results obtained by the X-ray microdiffraction showed that after some days and at room temperature urine increased significantly both amorphous and crystalline phases. (literal)
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