Pompon-like MnF 2 nanostructures from a single-source precursor through atmospheric pressure chemical vapor deposition (Articolo in rivista)

Type
Label
  • Pompon-like MnF 2 nanostructures from a single-source precursor through atmospheric pressure chemical vapor deposition (Articolo in rivista) (literal)
Anno
  • 2012-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.1002/ejic.201101121 (literal)
Alternative label
  • Malandrino, G., Toro, R.G., Catalano, M.R., Fragalà, M.E., Rossi, P., Paoli, P. (2012)
    Pompon-like MnF 2 nanostructures from a single-source precursor through atmospheric pressure chemical vapor deposition
    in European journal of inorganic chemistry (Print)
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Malandrino, G., Toro, R.G., Catalano, M.R., Fragalà, M.E., Rossi, P., Paoli, P. (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#url
  • http://dx.doi.org/10.1016/j.matchemphys.2012.02.024 (literal)
Rivista
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • Dipartimento di Scienze Chimiche, Università di Catania, ISTM-CNR, V.le Andrea Doria 6, 95125 Catania, Italy Istituto per Lo Studio Dei Materiali Nanostrutturati (ISMN), CNR Area della Ricerca di Roma, via Salaria Km 29.300, Monterotondo Stazione, Roma 00016, Italy Dipartimento di Energetica S. Stecco, Università di Firenze, via Santa Marta 3, 50136 Firenze, Italy (literal)
Titolo
  • Pompon-like MnF 2 nanostructures from a single-source precursor through atmospheric pressure chemical vapor deposition (literal)
Abstract
  • MnF 2 nanorod assemblies in a pompon-like fashion were synthesized by using a new complex, Mn(hfa) 2·tmeda [(Hhfa = 1,1,1,5,5,5-hexafluoro-2,4-pentandione, tmeda = N,N,N?,N?- tetramethylethylenediamine)]. The complex was synthesized in a single-step reaction, and single-crystal X-ray diffraction studies provide evidence of a mononuclear structure. The thermal analyses have shown that the complex is thermally stable and can be evaporated to leave less than 2 % residue at atmospheric pressure. On the basis of its thermal properties, it has been successfully applied to the atmospheric pressure metalorganic chemical vapor deposition (AP-MOCVD) of MnF 2 nanostructures. A mild approach, atmospheric pressure metalorganic chemical vapor deposition (AP-MOCVD), was applied for the fabrication of pompon-like assemblies of MnF 2 nanorods. Mn(hfa) 2·tmeda [(Hhfa = 1,1,1,5,5,5-hexafluoro-2,4- pentandione, tmeda = N,N,N?,N?-tetramethylethylenediamine)] was used as a single-source precursor (literal)
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