A solid state nuclear magnetic resonance study on the thermolytic synthesis of CdS nanoparticles in a polystyrene matrix (Articolo in rivista)

Type
Label
  • A solid state nuclear magnetic resonance study on the thermolytic synthesis of CdS nanoparticles in a polystyrene matrix (Articolo in rivista) (literal)
Anno
  • 2006-01-01T00:00:00+01:00 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#doi
  • 10.1016/j.matlet.2006.01.060 (literal)
Alternative label
  • Pentimalli M., Antolini F., Bauer E.M., Capitani D., Di Luccio T., Viel S. (2006)
    A solid state nuclear magnetic resonance study on the thermolytic synthesis of CdS nanoparticles in a polystyrene matrix
    in Materials letters (Gen. ed.)
    (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#autori
  • Pentimalli M., Antolini F., Bauer E.M., Capitani D., Di Luccio T., Viel S. (literal)
Pagina inizio
  • 2657 (literal)
Pagina fine
  • 2661 (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#numeroVolume
  • 60 (literal)
Rivista
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#note
  • http://dx.doi.org/10.1016/j.matlet.2006.01.060 (literal)
Note
  • ISI Web of Science (WOS) (literal)
Http://www.cnr.it/ontology/cnr/pubblicazioni.owl#affiliazioni
  • ENEA, UTS MAT C.R. Casaccia, Via Angguillarese 301, 00100 Roma, Italy; ENEA, UTS MAT CR Faenza,Via Ravegnana 186, 48018 Faenza, Italy; CNR-ISM, Italy; CNR IMC, Via Salaria Km 29,300, 00016 Monterotondo S., Roma, Italy; ENEA, UTS MAT CR Brindisi S.S. 7 Appia Km 713,7, 72100 Brindisi, Italy; University of Aix Marseille I and III, JE 2421 Traces, Site de Saint-Jerome, Service 511, 13397 Marseille, Cedex 20, France (literal)
Titolo
  • A solid state nuclear magnetic resonance study on the thermolytic synthesis of CdS nanoparticles in a polystyrene matrix (literal)
Abstract
  • We report on the optimization of the thermolytic synthesis of cadmium sulfide (CdS) nanoparticles in a polystyrene (PS) matrix. The annealing conditions were tuned on the basis of the indications coming from solid state 113Cd and 13C Nuclear Magnetic Resonance (NMR) experiments. 113Cd NMR provided direct evidence of CdS nanoparticles formation. Semi-quantitative 13C NMR experiments demonstrated that good quality samples are obtained by heating up precursor/polystyrene films to 270 °C in vacuum. X-ray diffraction (XRD) and wide angle X-ray scattering (WAXS) experiments revealed structural details of CdS nanoparticles, their average size ranging from 1 to more than 7 nm as a function of the annealing conditions. (literal)
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